Difference between revisions of "KJM5911 Lab Exercise 5 - Cyclotron Produced Tracers and Liquid-Liquid Extraction"
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Jonpo@uio.no (talk | contribs) (→Experimental Procedure) |
Jonpo@uio.no (talk | contribs) (→Experimental Procedure) |
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=== Experimental Procedure === | === Experimental Procedure === | ||
| − | Part 1: Producing 90Mo in a (alpha, 4n) reaction | + | '''Part 1: Producing 90Mo in a (alpha, 4n) reaction''' |
*Welcome to the Oslo Cyclotron Laboratory. | *Welcome to the Oslo Cyclotron Laboratory. | ||
*Target setup and gas-jet transfer system. | *Target setup and gas-jet transfer system. | ||
| Line 19: | Line 19: | ||
*Analysing the gamma spectrum | *Analysing the gamma spectrum | ||
| − | Part 2: Liquid-liquid extraction of Mo | + | '''Part 2: Liquid-liquid extraction of Mo''' |
*Preparing liquids and equipment. | *Preparing liquids and equipment. | ||
*Extraction curve as function TOA concentration. | *Extraction curve as function TOA concentration. | ||
| Line 25: | Line 25: | ||
**Plot extraction data and analyse curve | **Plot extraction data and analyse curve | ||
| − | Part 3: Clean up | + | '''Part 3: Clean up''' |
*Clean all equipment and collect rad. waste in designated bottles. | *Clean all equipment and collect rad. waste in designated bottles. | ||
*Prepare all waste for collection/disposal. | *Prepare all waste for collection/disposal. | ||
Revision as of 12:58, 18 October 2012
Learning Goals
Theory
Experimental Procedure
Part 1: Producing 90Mo in a (alpha, 4n) reaction
- Welcome to the Oslo Cyclotron Laboratory.
- Target setup and gas-jet transfer system.
- Catching 90Mo on a filter in the chem.lab.
- Analysing the gamma spectrum
Part 2: Liquid-liquid extraction of Mo
- Preparing liquids and equipment.
- Extraction curve as function TOA concentration.
- Perform extractions with 90Mo tracer
- Plot extraction data and analyse curve
Part 3: Clean up
- Clean all equipment and collect rad. waste in designated bottles.
- Prepare all waste for collection/disposal.
- Check workspace for contamination.
